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Beilstein J. Org. Chem. 2016, 12, 1302–1308, doi:10.3762/bjoc.12.122
Graphical Abstract
Figure 1: Tetraphenylene and its saddle-shaped structure.
Scheme 1: The Pd(OAc)2-catalyzed reaction of nitriles with tetraphenylene (1).
Beilstein J. Org. Chem. 2014, 10, 2071–2076, doi:10.3762/bjoc.10.215
Scheme 1: C–H functionalization of P(O)R2 directed through a seven-membered cyclopalladium transition state.
Scheme 2: Synthesis of chiral and racemic substrates.
Figure 1: C–H functionalization of axially chiral phosphorus substrates. The yields are isolated yields and t...
Beilstein J. Org. Chem. 2013, 9, 1179–1184, doi:10.3762/bjoc.9.132
Figure 1: Lyconadin A.
Scheme 1: Retrosynthetic analysis of 1.
Scheme 2: Synthesis of triether 15.
Scheme 3: Synthesis and attempted ring-opening of epoxide 17.
Scheme 4: Attempted protection of 14 and silyl migration.
Scheme 5: Synthesis and ring-opening rearrangement of epoxide 25.
Scheme 6: Proposed mechanism for generation of alcohol 26.
Scheme 7: Synthesis of epoxide 29 from alcohol 26 (asterisks indicate relative but not absolute stereochemist...